Jingshe Song, Ph.D.

**** ******** *****, ***** ****, TX77479

Cell: 281-***-**** E-mail: ac0rr2@r.postjobfree.com

SUMMARY

An upstream and downstream Chemicals R&D Scientist won several hundred millions businesses for Nalco and Baker Hughes

An expert in polymer synthesis and polymer structure-property relationships Successful research career in polymer chemistry and colloidal chemistry As the leading scientist, developed the best cost-effective products such as friction reducers (polymer dispersion and inverse emulsion), viscosifier, delayed and instant crosslinker, polymeric crosslinker, hydrogen sulfide scavenger, corrosion, paraffin, and scale inhibitors Comprehensive knowledge in oil & gas industry, cementing, acidizing, fracturing, drilling fluids, downstream and upstream chemicals

PROFESSIONAL EXPERIENCE

2014.1-2017.4 Project Manager, Baker Petrolite LLC Baker Hughes Energy Services Division, Sugar Land, TX77478 Achievements:

Developed the most cost effective hydrogen sulfide scavenger. Improved the suspension stability of oil-soluble polyolefin friction reducer. Developed the self-release coating for reactors and for Ziegler –Natta catalysts. Developed a high quality water-based emulsion for oil-soluble friction reducer. Developed a viscoelastic surfactant (VES) fluid for acidizing for high temperature application.

Developed a VES compatible corrosion inhibitor for acidizing. Developed and scaled up polyacrylamide emulsion for acidizing viscosifier and friction reducer.

2008.8-2014.1 Senior Research Chemist in Nalco Champion Technologies Energy Services Division, Sugar Land, TX77478

Achievements:

Developed new polymers for oil & gas well stimulation and enhanced oil recovery applications.

Solved the long-existing problems in the manufacturing of Nalco Ultimer product (polymer dispersion in brine, won USA Presidential Award) by redesigning the formulation and the reaction conditions. Scaled up the dispersion polymerization (for Ultimer product) from 1 lb to 100,000 lbs per batch.

Developed low cost fast-inverting inverse emulsion applied as friction reducers for heavy brines and produced field waters.

Developed a new method of micellar polymerization for hydrophobically associative polymers. Decreased the usage of surfactant by 93% and improved the sand suspension performance significantly (applied in hydraulic fracturing for oil and natural gas).

Developed a new method for Ulexite suspension in aqueous solution applied for delayed crosslinker and instant crosslinkers.

Developed a new chemistry of polymeric crosslinker applied in Guar gel which Jingshe Song, Ph.D., University of Toronto

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could decrease the Guar usage by 50%.

2006.11-2008.6 NSERC Fellowship in National Research Council of Canada Research Associate from August 2007

Institute for Chemical & Environmental Technology, NRC, Ottawa, Canada Achievements:

Developed a new process to synthesize ladder polymers with high molar mass by condensation polymerization.

Modified polymer by chemical reactions.

Studied film formation process.

2006.08-2006.11 Post-doctor research chemist

University of Toronto, Toronto, Canada

Achievements:

Developed a novel robust process for preparing lanthanide (La, Eu, Ho) inorganic nanoparticles with controlled particle diameter from 3 nm to 30 nm. Incorporated these inorganic particles into polymeric particles by emulsifier- free emulsion polymerization, emulsion, miniemulsion and dispersion polymn. 2002.-2006.07 PhD candidate, Polymer Chemistry and Colloidal chemistry Chemistry department, U of Toronto, Canada

Achievements:

Developed a new robust process for preparing monodisperse functionalized polymer microspheres.

Carried out dispersion polymerization; miniemulsion polymerization; emulsion polymerization; suspension polymerization.

Carried out free radical polymerization; living radical polymerization. Studied photostability of organic dyes in polymer particles. 2000.11-2001.10 Research chemist or process engineer, worked for Bayer company Department of Chemical and Biochemical Engineering, University of Western Ontario, Canada

Achievements: Carried out living carbocationic polymerization to prepare and characterize hydroxyl-functionalized polymers or telechelic polymers. Developed a new method to synthesize inimer for hyperbranched polymer. 1995-2000 Assistant professor, promoted to associate professor in 2000 Qingdao University of Science & Technology, China

Achievements: Carried out coordination anionic polymerization, solution polymerization, bulk precipitation polymerization. Polymer formulations and applications.

Developed a new process for trans-1, 4-polyisoprene manufacturing, which reduced its production cost by 90%.

1990.07-1992.08 Assistant engineer

Qilu Petrochemical Research Centre, China Petrochemical Company, Zibo, China Achievements: Developed two types of novel rubber/plastic blends. Jingshe Song, Ph.D., University of Toronto

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SPECIAL SKILLS

● 9 years of research experience in upstream/dowstream chemicals.

● More than 15 years of research experience in the field of polymer chemistry and advanced materials.

● Excellent in the synthesis of polymers by free radical, cationic and coordination anionic, and condensation polymerization.

● Skilled in living polymerization.

● Skilled in organic synthesis.

● Expert in emulsification process and emulsion polymerization.

● Skilled in dispersed formulations and processes, and scale-up.

● Excellent in problem solving, research analysis, decision making, innovation and leadership skills.

● Experienced in handling industrial research projects and different chemical testing equipment.

● Experienced in the preparation, modification and characterization of monodispersed microspheres.

● Experienced in the preparation and applications of polymer materials

● Capable of polymer compound design and testing.

● Skilled in preparing technical reports.

● Able to work independently or in a team.

● Excellent in documentation, communication, presentation and interpersonal skills.

● Committed to continuous learning and improvement. EDUCATION

2002-Aug 2006 Ph.D. in Science, Polymer Chemistry

University of Toronto, Canada,

Thesis: Synthesis of Micron-size Monodisperse Functional Polymeric Microspheres by Two-stage Dispersion Polymerization Thesis advisor: Mitchell A. Winnik

1992-1995 Master of Science, Polymer Chemistry and Material Science, Qingdao University of Science & Technology, China

Thesis: Synthesis, characterization and application of trans-polyisoprene by coordination precipitation Polymerization

1986-1990 Bachelor of Science, Polymer Materials and Chemical Engineering Qingdao University of Science & Technology, China

HONORS

2010

2006-2008

Nalco Company Team Award

NSERC Fellowship in National Research Council of Canada 2006 2005 MSED/LANXESS Graduate Research Award in Polymer Science and Engineering

2005 ICI graduate research award, finalist of PMSE competition, in Polymeric Materials Science and Engineering

2005-2006 Robert & Jean Hadgraft Graduate Fellowship Award in Chemistry Jingshe Song, Ph.D., University of Toronto

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2005-2006 Ontario graduate scholarship (OGS)

2005-2006 J. Warren Flanagan scholarship in Chemistry 2005-2006 UTF Conference Travel Grant

2002-2005 University of Toronto Scholarship

2003-2004 Ontario graduate scholarship (OGS)

2000 Scientific and Technological Invention Award in China (highest invention award in 2000)

1999 Scientific and Technological Invention Award of Chemical Industry Ministry in 1999. Jingshe Song, Ph.D., University of Toronto

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Patents, Publications and Presentations

PATENTS

1. Metal-based hydrogen sulfide and method of preparing same 2016 2. VES-compatible corrosion inhibitor 2016

3. Self-releasing coating for FLO polymer reactors 2016 4. Gel breaking system for VES acidizing fluids 2015 5. Temperature sensitive viscoelastic well-treatment fluids 2014, US2014262293 (A1) US9228123 (B2) WO2014164078 (A1) EP2970747 (A1) EP2970747 (A4) CN105073944 (A) CA2904637 (A1)

6. Choline-based crosslinker compositions for fracturing fluids 2013 US201361810498P 20130410 ; WO2014US33511 20140409

7. Reversible crosslinked water-soluble polymers for oil field application. 2010 8. Carboxylated Polymers of Intrinsic Microporosity (PIMs) with Tunable Gas Transport Properties

US20090213031P 20090430; WO2010CA00323 20100310 ; US201013266304 20100310 9. Process of making monodisperse, controlled-size micrometer polymer particles, WO05026225A1, (Application time: Nov. 2003)

10. Fine quality tyre rubber material containing rich trans-1,4-polyisoprene CN1997115171 19970728

11. Synthesis of homotrans-1,4-polyisoprene, 1996, CN 1117501. 12. Synthesis of epoxidized trans-1,4-polyisoprene, 2001, CN 1292388 13. The Cable Jacket Material of Linear Low-density Polyethylene, 1992, CN 1074779A PUBLICATIONS

1. Du, N.Y., Robertson, G.P., Song, J.S., Pinnau, I., and Guiver, M.D. High-Performance Carboxylated Polymers of Intrinsic Microporosity (PIMs) with Tunable Gas Transport Properties, Macromolecules, 2009, 42, 6038-6043.

2. Du, N.Y., Song, J.S., Guiver, M.D. Linear High Molecular Weight Ladder Polymer via Fast Polycondensation of 5, 5’, 6, 6’-Tetrahydroxy-3, 3, 3’, 3’-tetramethylspirobisindane with 1, 4- Dicyanotetrafluorobenzene, Macromolecular Rapid Communications, 2008, 29, 783-788. 3. Du, N.Y., Robertson, G.P., Song, J.S., Pinnau, I., Thomas, S., Guiver, M.D. Polymers of Intrinsic Microporosity Containing Trifluoromethyl and Phenylsulfone Groups as Materials for Membrane Gas Separation, Macromolecules, 2008, 41, 9656-9662. 4. Song, J.S., Du, N.Y., Guiver, M.D. Linear Ladder Polymers by Optimizing Condensation Polymerization of Tetrahydroxytetramethylspirobisindane and 1,4-dicyanotetrafluorobenzene, Macromolecules, 2008, 41, 7411-7417.

5. Song, J.S. and Winnik, MA, Monodisperse, micron-size reactive oligomer particles by two- stage living radical dispersion polymerization, Macromolecules, 2006, 39, 8318-8325. 6. Song, J.S. and Winnik, MA, Preparation of carboxyl-functionalized monodisperse, spherical controlled-size micrometer polymer particles by two-stage dispersion polymerization, Macromolecules, 2006, 39, 5729-5737.

7. Song, J.S. and Winnik, MA, Dye-labeled monodisperse, spherical controlled-size micrometer polymer particles by two-stage dispersion polymerization, Polymer, 2006, 47, 817-825. 8. Song, J.S. and Winnik, MA, Monodisperse low molar mass micron-size polymer particles by two-stage dispersion polymerization, Polymer, 2006, 47, 4557-4563. Jingshe Song, Ph.D., University of Toronto

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9. Song, J.S. and Winnik, MA, Cross-Linked, Monodisperse, Micron-Sized Polystyrene Particles by Two-Stage Dispersion Polymerization, Macromolecules, 2005, 38, 8300-8307. 10. Song, J.S. and Winnik, M.A., Synthesis of Functional Monodisperse Polymeric Microspheres by Two-stage Dispersion Polymerization, ACS national meeting, PMSE Preprints, 2005, 93, 314-315.

11. Song, J.S.; Tronc, F.; and Winnik, MA, Two-stage dispersion polymerization towards monodisperse micron-size copolymer particles, J. Am. Chem. Soc. 2004, 126, 6564. 12. Song, J., and Puskas J.E., Direct Functionalization of Polyisobutylene by Living Initiation with Methylstyrene Epoxide J. Polym. Sci., Polym. Chem. Ed., 2002, 40(8), 1005-1015. 13. Song, J.S. and Huang B.C., Progress and Synthesis and Application of Trans-1,4-polyisoprene, J. Appl. Polym. Sci., 2001, 82(1): 81-89.

14. Song, J.S., Ma, Z.W., Huang, B.C., (2002) Aftertreatment and Aging of Trans-1,4- Polyisoprene, China Synthetic Rubber Industry; 25(3):154-157. 15. Song, J.S., Ma, Z.W., Huang, B.C., (2002) The Control of Molecular Weight of Trans-1,4- polyisoprene, China Synthetic Rubber Industry 25(1):24-27. 16. Ma, Z.W., Song, J.S., Huang, B.C., (2001) Processing behavior of Trans-1,4-polyisoprene, China Synthetic Rubber Industry 24(4):22.

17. Feng, Y.H., Song, J.S., Huang, B.C., (2000) Bulk Polymerization of Butadiene and Copolymerization of Butadiene with Isoprene, China Synthetic Rubber Industry 23(4), 222. 18. Feng, Y.H., Song, J.S., Huang, B.C., (1999) Synthesis of High Trans-1,4-polybutadiene with Slurry Polymerization, China Synthetic Rubber Industry, 22(5), 276. 19. Song, J.S., Fan, R.L., Huang, B.C., Feng, M., Tian, B., Yao, W, (1999) Processing and Application Properties of Tire Stocks Containing Trans-1,4-polyisoprene, China Tire Industry, 19,9.

20. Song, J.S., Huang, B.C., Zhang, H., Yao, W, (1998) Blending of High Trans-1,4-Polyisoprene and Polyethylene, Plastics Science and Technology, 127(5), 4. 21. Huang, B.C., Song, J.S., Yao, W., Feng, Y.H., (1998) Development of Research on Trans-1,4- Polyisoprene Rubber, China Chemical Technology, (7), 39. 22. Song, J.S., Huang, B.C., He, J.D., Yao, W., (1998) Bulk Precipitation Polymerization Kinetics of Isoprene with Supported Titanium Catalyst, China Synthetic Rubber Industry, 21(5):292. 23. Song, J.S., Huang, B.C., Zhang, H., Yao, W. (1998) Study of TPI/PP Blend System by Dynamic Vulcanization, China Plastics Industry, 26(2): 119. 24. Song, J.S., Huang, B.C., Pan, R.S., Yao, W., (1998) Research on Shape Memory Material of High Trans-1,4-Polyisoprene, China Elastomerics, 8(1): 1. 25. Song, J.S., Huang, B.C., Fan, R.L., Yao, W., (1997) Study on Vulcanizates of Trans-1,4- Polyisoprene and Its Blends, China Rubber Industry, 44(4): 209. 26. He, J.D., Song, J.S., Huang, B.C., Synthesis, Structure and Properties of Trans-1,4- Polyisoprene, Journal of Qingdao Institute of Chemical Technology 1995;16(3):288. 27. Yao, W., Song, J.S., He, A.H., Huang, B.C., Vulcanization and Properties of Synthetic Trans- 1,4-Polyisoprene, China Elastomerics, 1995; 5(1):6. 28. Yao, W., He, A.H., Song, J.S., Huang, B.C., Crystallization Behavior of Trans-1,4- Polyisoprene, China Synthetic Rubber Industry, 1996; 19(5):287. PRESENTATIONS

1. Michael D. Guiver; Naiying Du; Gilles P. Robertson; Jingshe Song; Sylvie Thomas; Ingo Pinnau; Michael D. Guiver, Novel Polymers of Intrinsic Microporosity for Membrane Gas Separation, invited presentation given by Michael D. Guiver. 237th ACS Spring National Meeting and Exposition, March 22 – 26, 2009, Salt Lake City, UT, USA. Jingshe Song, Ph.D., University of Toronto

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2. Ingo Pinnau; Sylvie Thomas; Michael D. Guiver; Naiying Du; Jingshe Song, Mixed-Gas Transport Properties of Microporous Polymers, presentation given by Ingo Pinnau at the Inaugural Mexican-American Conference on Advances in Polymer Science, December 7 – 10, 2008 Los Cabos, Mexico.

3. Juhyeon Ahn; Wook-Jin Chung; Ingo Pinnau; Naiying Du; Jingshe Song; Michael D. Guiver, Gas Transport Behavior of Membranes Composed of Silica Nanoparticle in Polymers of Intrinsic Microporosity (PIM), poster presented at the International Congress on Membranes and Membrane Processes (ICOM). July 12 – 18, 2008, Honolulu, Hawaii, USA. 4. Song, J.S. and Winnik M.A., (2006) Synthesis of Carboxylated Monodisperse Polymeric Microspheres by Two-stage Dispersion Polymerization, 89th Canadian Chemistry Conference and Exhibition, May. 27-31. Halifax, Canada. (Ph. D. work, Invited oral presentation, MSED/Lanxess Award)

5. Song, J.S. and Winnik M.A., (2005) Synthesis of Functional Monodisperse Polymeric Microspheres by Two-stage Dispersion Polymerization, 230th ACS National meeting, Aug. 28- Sep. 1. Washington DC, USA (Ph. D. work, Invited oral presentation, finalist of PMSE competition)

6. Song, J.S., and Winnik M.A., (2005) Synthesis of Micron-size Monodisperse Carboxyl- Functional Polymeric Microspheres by Two-stage Dispersion Polymerization, Gordon Research Conference, Polymer Colloids, July, Tilton, USA (Ph. D. work) 7. Winnik, M.A. Song, J.S., (2005) The Synthesis of Functional Polymeric Microspheres by Two-stage Dispersion Polymerization, 2nd International Symposium on Polymeric Microspheres program page April, 2005, Japan (Ph. D. work, Oral presentation by Prof. Winnik)

8. Song, J.S., and Winnik M.A., (2004) Controlled Micron-size Monodisperse Copolymer Particles by Two-stage Dispersion Polymerization, MSE Conference, June, Ottawa, Canada

(Ph. D. work)

9. Song, J.S., and Winnik M.A., (2004) Monodisperse, Carboxyl-Functional, Controlled Micron- Size Particles by Two-stage Dispersion Polymerization, 87th Canadian Chemistry Conference and Exhibition, May, London, Canada. (Ph. D. work) 10. Song, J.S., and Winnik MA, (2003) Synthesis of HY-labeled Polymer Particles by Mini-emulsion Polymerization, Gordon Research Conference, Polymer Colloids, July, Tilton, USA (Research chemist in UofT)

11. J.E.Puskas, J.Song, Y. Chen: Synthesis and Characterization of α,ω-Dihydroxyl-Telechelic Polyisobutylene via Living Carbocationic Initiation and Coupling. Paper#7, ACS Rubber Division, 163nd Technical Meeting, April 28-30, San Francisco, CA (2003) 12. Fan, R.L., Song, J.S., Huang, B.C., Shi, X.Z., (1997) International Rubber conference Malasia P469

13. Huang, B.C., Song, J.S., Zhang, H., (1997) International Rubber Conference, Malasia P999 14. Huang, B.C., Song, J.S., (1996) 36th IUPAC International symposium on Macromolecules, Aug. 4-9 Korea,

15. Song, J.S., Ma, Z.W., Huang, B.C., Yao, W., Feng, Y.H., The Control of Molecular Weight of Trans-1,4-polyisoprene, Conference in New Material Area of China High Technology, 1998.9 Chengdu, P13-16

16. Song, J.S., Ma, Z.W., Huang, B.C., etc., Aftertreatment and Aging of Trans-1,4-Polyisoprene, Conference in New Material Area of China High Technology, 1998.9 Chengdu, P8-12 Corporation reports

Jingshe Song, Ph.D., University of Toronto

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1. For Nalco Company, Song, J.S., Temperature-tunable hydrophobically water-soluble polymers for oil field application. 2009

2. For Nalco Company, Song, J.S., Reversible crosslinked water-soluble polymers for oil field application. 2009

3. For Nalco Company, Song, J.S., Process improvement for Reversible crosslinked water- soluble polymers for oil field application. 2008

4. For Clariant international Ltd, Song, J.S. and Winnik, MA, Synthesis and photostability of Hostasol Yellow-incorporated particles by miniemulsion polymerization, 2003 5. For Clariant international Ltd, Song, J.S. and Winnik, MA, Compatibility and photostability of Hostasol Yellow-incorporated polymer with high density polyethylene, 2003 6. For Bayer company, J. Song, J.E.Puskas: Report #21, Bayer Contract, September 15, 2001 (30 pp).

7. For Bayer company, Y. Kwon, J. Song, J. Bodis, J.E. Puskas: Report #19, Bayer Contract, June. 30, 2001 (22pp)

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