Dr. R. Dileep
#****, ***** *** *-******** Mobile: +91-988*******
9th Block Jayanagar Email: **********@*****.***
Bangalore-560069 ******.***@*****.***
Objective
To seek a position in a challenging field which can give me an opportunity to unleash my potential and replenish a good learning experience.
Profile
Excellent theoretical, experimental and communication skills
Having ability to use education and experience in the field of Chemical Science.
Motivated towards challenging research.
Educational Background
Ph.D.
Title: Studies on Catalytic Oxidation of Alcohols Using Transition Metal Complexes
Institute: National Institute of Technology Karnataka, Surathkal, Mangalore,
India.
Advisor: Dr. B. Ramachandra Bhat
Year: 2007- 10
M.Sc. (Chemistry)
Project: Quantative analysis of promethazine hydrochloride using sodium chlorite
Institute: University of Mysore, Manasagangotri, Mysore, India
Advisor: Dr. K. Basavaiah
Year: 2002-04
Research Experience
Various chemical reactions including oxidation, reduction and other chemical complex reactions involving ring opening, cyclization, hydroboration, condensation, halogenation, sulfonation, organometallic reactions, dealkylation, debenzylation, hydrogenation etc.
Synthesis and characterization of transition metal complexes including organometallic compounds
Studies on homogeneous and heterogeneous catalytic reactions
Having good skill of elucidating the structure from FTIR, NMR, Mass and Elemental analysis data.
Having profound instrument operating knowledge of HPLC, LC-MS, GC, GC-MS, NMR, FTIR, UV-Visible, Fluorescence, CHNS analyzer, Auto titrator, total organic carbon analyzer, particle size analyzer and Brooksfield Viscometer.
Professional Experience
Merck Millipore India Pvt. Ltd., Bangalore
[Sep 2010- Jan 2012]
Access specialist, Extractable Lab
Responsibilities
Establishing and development of Analytical laboratory for Extractables and Leachables analysis
Method development and Experimental design for Extractables and Leachables testing.
Quantification and Identification of Extractables and Leachables in drug products.
Identification of Impurities in products and their quantification.
Chemical compatibility studies for the different types of organic polymers.
Antibiotic binding studies for different types of organic polymeric filters.
Filter validation studies (Physical Testing-bubble point and compatibility testing)
Customer communication in terms of answering to queries from regulatory.
Analytical documentation, preparation of protocols and reports.
Non- routine analysis leading to innovation and publication
Calibration of analytical instrumentation.
Dr Reddy Laboratories, Hyderabad
[Nov 2005– June 2007]
Junior Manager (Analytical R &D)
Responsibilities:
Literature search, analytical method development and validation of new APIs and finished products
Stability studies of finished products
Instrument calibration-HPLC, GC, UV-Vis spectrophotometer, FTIR, Auto-titrator and dissolution apparatus
Hikal Limited, Bangalore
[June 2004 - Nov 2005]
Senior Chemist
Responsibilities:
Analytical method development and validation of new active pharmaceutical ingredients (API)
Stability studies of APIs
Instrument calibration-HPLC, GC, UV-Vis spectrophotometer, FTIR, Auto-titrator
Process Validation and cleaning validation
Awards & Achievements
o Played a major role in the set up and qualification of an analytical lab for Extractables Studies at Merck Millipore India pvt. Ltd., Bangalore.
o Qualified CSIR-NET examination (June 2007)
o Award for highest marks in Chemistry in B.Sc
o Prizes won for lectures and debates in Chemistry, History and Psychology.
Research Interests
• Catalysis
• Reagents in Organic synthesis
• Materials for Non-Linear Optical applications
• High energy materials
• Synthetic organic & Inorganic Chemistry for Biological applications
• Coordination and organometallic Chemistry.
• Analytical Chemistry and Instrumentation
Publications, Conferences and Workshops
Research papers published in journals
[1] Dileep Ramakrishna and Badekai Ramachandra Bhat (2010). “Cobalt complexes in [EMIM] Cl – A catalyst for oxidation of alcohols to carbonyls”. Inorg. Chem. Commun., 13, 195-198.
[2] Dileep Ramakrishna, Badekai Ramachandra Bhat and Ramasamy Karvembu (2010). “Catalytic oxidation of alcohols by nickel (II) Schiff base complexes containing triphenylphosphine in ionic liquid: An attempt towards green oxidation process”. Catal. Commun. 11, 498-501.
[3] Dileep Ramakrishna and Badekai Ramachandra Bhat (2010). “Palladium-Schiff base-triphenylphosphine catalyzed oxidation of alcohols” Applied Organomet. Chem., 24, 663-666.
[4] Dileep Ramakrishna and Badekai Ramachandra Bhat (2010) “Effective oxidation of alcohols with H5IO6 catalyzed by Nickel (II)-Schiff base complexes”. Synth. React. Inorg. Met.-Org. Nano-Met. Chem., 40, 516-520.
[5] Dileep Ramakrishna and Badekai Ramachandra Bhat (2011). “Ruthenium Green Conversion of Alcohols to Carbonyls Catalyzed by Novel Ruthenium-Schiff base-triphenylphosphine complexes.” Inorg. Chem. Commun. 14, 155-158.
[6] Dileep Ramakrishna and Badekai Ramachandra Bhat (2011). “A catalytic process for the selective oxidation of alcohols by copper (II) complexes.” Inorg. Chem. Commun., 14, 690-693.
[7] A.S. Ramasubramanian, B. Ramachandra Bhat and R. Dileep (2010) “Synthesis, characterization and applications of metal complexes of 5-Nitrosalicylidene 4-amino 3-mercapto-1, 2, 4-triazine- 5-one” Rasaayan J. Chem. 3, 122-126.
[8] A.S. Ramasubramanian, B. Ramachandra Bhat and R. Dileep (2010). “Synthesis characterization and biological activity of metal complexes of 4-ethyl vanillideneamino-3-methyl-5-mercapto-1, 2, 4-triazole.” J. Coord. Chem., 63, 3108-3116.
[9] Rudresha Bada Jayappa, Badekai Ramachandra Bhat, Dileep Ramakrishna, John Kiran Anthony and Fabian Rotermund (2010). “Third-order optical nonlinear studies of Cobalt (II) Schiff base complex bearing triphenylphosphine using Differential Optical Kerr Gate and Z-scan techniques.” Synth. Met. 160, 1584-1586.
[10] A.S. Ramasubramanian, B. Ramachandra Bhat, R. Dileep and Sandya Rani (2011). “Transition metal complexes of 5-bromosalicylidene-4-amino-3-mercapto-1,2,4-triazine-5-one: Synthesis, characterization, catalytic and antibacterial studies” J. Serb. Chem. Soc.76, 75 – 83.
[11] A.S. Ramasubramanian, B. Ramachandra Bhat and R. Dileep. “Thermal and antibacterial studies of novel Lanthanide Schiff base complexes.” Accepted for publication in Synth. React. Inorg. Met.-Org. Nano-Met. Chem
[12] Rudresha Bada Jayappa,Badekai Ramachandra Bhat, Dileep Ramakrishna, J. K. Anthony, H.W. Lee and F.Rotermund (2012), Nonlinear optical study of palladium Schiff base complexsing femtosecond differential optical Kerr gate and Z- scan techniques, Optics and Laser Technology, 44, 1180-1183.
[13] Ramakrishna Dileep, Badekai Ramachandra Bhat and T. N. Guru Row. “Palladium complexes for catalytic oxidation of alcohols in ionic liquid.” Communicated to Inorg. Chim. Acta (Minor Revision).
[14] Dileep Ramakrishna and Badekai Ramachandra Bhat. “Catalytic oxidation of primary and secondary alcohols by Cobalt (II) Schiff base complexes.” Communicated to Synth. React. Inorg. Met.-Org. Nano-Met. Chem.
[15] Rudresha Bada Jayappa, Badekai Ramachandra Bhat and Dileep Ramakrishna. “Large and Ultrafast Third-Order Optical Nonlinearity of Palladium (I) Complex.” Communication to Opt. Commun. (Under review).
[16] A.S. Ramasubramanian, B. Ramachandra Bhat, R. Dileep and Sandya Rani. “Complexing behaviour of NNO donor Schiff base ligand with transition metal ions and their applications.” Communicated to J. Coord. Chem.
[17] Dileep Ramakrishna and Badekai Ramachandra Bhat. “Selective oxidation of alcohols by copper (II) complexes”. Manuscript under preparation
[18] Dileep Ramakrishna and Badekai Ramachandra Bhat. “Catalytic oxidation of primary and secondary alcohols by Ru(II) Schiff base complexes.” Manuscript under preparation
Conferences
[1] Dileep. R, Nagaraj.K, Ritesh.P, Vinay.S.K and Ramachandra Bhat. B. “Synthesis and Characterization of Ni (II) complex with 4-Vanillidenamino-3-methyl-5-mercapto 1, 2, 4-triazole”. Presented at the 27th Annual conference of the Indian Council of Chemists (ICC-08) held at H. S. Gaur University, Sagar on 26th-28th February 2008.
[2] Dileep R, R. Karvembu and B. Ramachandra Bhat. “Homogeneous catalytic oxidation of alcohols using Ni (II) complexes”. Presented at the International Conference on Frontiers in Chemical Research (ICFCR-2008) held at Mangalore University on 29th-31st December 2008.
[3] Dileep R and B. Ramachandra Bhat. “Synthesis, crystal structures and spectral studies of Palladium (II) complexes containing NNO donor Schiff base and Triphenylphosphine” Presented at the 27th Annual conference of the Indian Council of Chemists (ICC-08) held at Gurukul Kangri Vishwavidyalaya, Haridwar on 26th-28th December 2008
[4] Dileep R and B. Ramachandra Bhat. “Catalytic oxidation of alcohols to carbonyl compounds by Co(II) complexes Containing NNO donor Schiff base and triphenylphosphine”. Presented at the International Conference on Coordination and Organometallic Chemistry, held at Bharatiar University, Coimbatore on 19th and 20th March 2009.
[5] A.S. Ramasubramanian, R. Dileep and B. Ramachandra Bhat. “Synthesis, characterization and applications of metal complexes of 4-ethylvanillidene-amino-3-methyl-5-mercapto-1,2,4-triazole”. Presented at the 23rd International Conference on Organometallic Chemistry 2008, Rennes, France on 13th-18th July, 2008.
[6] Dileep R and B. Ramachandra Bhat. “Copper complexes for catalytic oxidation of alcohols in ionic liquid”. Presented at the International Conference on Emerging Trends in Chemistry, held at University of Pune, Pune on 5th-7th January 2010.
[7] Dileep R and B. Ramachandra Bhat. “Ruthenium-Schiff base-triphenylphosphine complexes: Synthesis, characterization, catalytic and kinetic studies”, presented at the National Conference on Recent trends in Chemical Research , held at National Institute of Technology Karnataka, Surathkal on 8th-10th March 2010.
Workshops
Attended three-day national workshop on “Modern Electro-chemical Techniques in Synthesis and Characterization of Advanced Materials (METSCAM-08)” organized by National Institute of Technology Karnataka, Mangalore.
Attended three-day national workshop on “Advances in Coordination Chemistry (ACC-09)” organized by National Institute of Technology Karnataka, Mangalore.
Attended three-day national workshop on “Advances in Organic Chemistry and Allied Applications (AOCAA 09)” organized by National Institute of Technology Karnataka, Mangalore.
Personal Details
Date of Birth : 17-02-1982
Marital Status : Married
Sex : Male
Father’s Name : A. Ramakrishna
Nationality : Indian
Languages Known : English, Telugu, Kannada, Hindi and Tamil.
Permanent address : #1530, Southend B-main road
9th Block, Jayanagar
Bangalore-560069
Karnataka, India.
References
Dr. B. Ramachandra Bhat Dr. R. Karvembu
Associate Professor Assistant Professor
Department of Chemistry Department of Chemistry
NITK Surathkal NIT Trichy
Srinivasanagar-575025 Tiruchirappalli-620015
***********@*****.*** ********@**********.***
Dr. Arun Mohan Isloor
Associate Professor
Department of Chemistry
NITK Surathkal
Srinivasanagar-575025
******@*****.***
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