Quality Assurance Control

Resume for Shad Mian.

***** ***** **** *****, *******, Texas 77047, Preferred Phone # 832-***-****, Email: rfl0il@r.postjobfree.com

OBJECTIVE: Seeking a position for a Chemist / Lab Tech

SUMMARY OF QUALIFICATIONS:

• Participated in Lab Safety programs and audits, safety of lab techs, equipment and chemical storage.

• I have used ASTM, IP, UOP methods.

• I have experience in physical and analytical testing in petrochemical labs.

• I am proficient with Microsoft Word, Excel and Power Point.

• I am experienced in multi-tasking and time- management while running the samples.

• Performed routine and non routine tests, reported results via LIMS and created certificate of analysis.

• I was involved in the development of new methods, writing sop’s, calibrations and quality assurance /quality control activities and training.

Participated in ISO audits in 1996, 2004, 2008 and internal and external audits in 2010

EMPLOYMENT

May 2010 – March 2011: Certispec USA, Texas City (Contract Position) – Lab Supervisor.

This was mainly an inspection company with a small laboratory. My responsibility as a lab supervisor was to help the lab techs in their daily activities. I also ordered lab supplies, created work-sheets and Certificates of Analysis. My responsibility was to make sure all the samples are analyzed as per the specifications provided by customers.

I have analyzed Waste Water Samples for Oil and Grease, Dead Bottoms Samples for Bacteria Check, Total Sediments in Residual fuels, Methanol Wall Wash and many more tests. I was involved in the preparation of ISO audit.

Aug 2007-Oct 2008: Camin Analytical Center, Pasadena Texas (Contact Position) – Lab Tech

I have tested the following products: Gasoline, Diesel, Bio-diesel, Jet Fuels, Crude Oils, & Other Petrochemicals. I have performed the following tests: RVP, Distillation, Cu strip, Nace corrosion, Gums, Doctor test, Mercaptan, Sulfur, Benzene (D3606), Oxygenates (D4815), Aromatics (GC-MS and DCPD D5569), Flash pt, Pour and Cloud pt, CFPP, Dupont, Ash, Carbon residue, Viscosity, Water by Karl Fisher, Water by Distillation, BS&W, Sediments, Salt in crude, Lubricity, Smoke point, Oxidation stability, Freeze point. Entered data in LIMS and produced a Certificate of Analysis.

A detailed list of the instruments and necessary glassware used to perform the testing are listed on the next page.

Dec 2001-Aug 2007: Inspectorate, Houston, Texas – Lab Tech

I was involved in the physical and analytical testing of the following products: Crude oil, fuel oil, VGO, gasoline, diesel, jet fuel, and bio-diesel samples. Tested the samples for copper and silver corrosion, nace corrosion, viscosities, water by distillation, API, smoke point, sediments, ash, sulfated ash, rvp, distillation, saybolt color, astm color, pt-co color, haze reading, appearance, odor, sulfur, nitrogen, chloride, iodine value, benzene, oxygenates, aromatics. I have used gas chromatographs, HP-5880, Chem. Station and GCMS. Also analyzed RR samples. .

A detailed list of the instruments and necessary glassware used to perform the testing are listed on the next page.

Mar 1978-May 1997: Shell Chemical Company, Deer Park, Texas – Lab Tech

Analyzed C2=, C3=, BB, BD, IP, DCPD, LPG, and water; to make sure the performance of the plant is safe and the environments are clean. Cross trained in Olefins, Environmental, Intermediates and Solvents laboratories to become more adaptable and valuable to the company. I coordinated health and safety issues in the lab to prevent injuries and practice safety at work and home. Also did water, asphalt and GC analysis for olefins samples. I maintained the QC and calibration program for the QC Lab. I was involved in the preparation of ISO audit in 1990.

Education: BS - Chemistry

Work Status: I am a USA Citizen

A detailed list of the methods, instruments and necessary glassware used to perform the testing are listed below:

D 56 Flash Point Closed Cup (Jet Fuel)

D 70 API Gravity (Pycnometer)

D 86 Distillation

D 93 Flash Point Closed Cup, Procedure A & B

D 95 Water by Distillation

D 97 Pour Point

D 130 Copper Strip - Corrosiveness to copper from Petroleum Products

D 156 Saybolt Color of Petroleum Products

D 189 Conradsom Carbon Residue

D 287 API Gravity (Hydrometer)

D 381 Motor Gases Unwashed & Washed Gums

D 445 Kinematic Viscosity of Transparent and Opaque Liquids

D 473 Sediments (Thimble) in Crude and Fuel Oils by Extraction Method

D 482 Ash from Petroleum Products

D 524 Ramsbottom Carbon Residue of Petroleum Products

D 525 Oxidation Stability - Induction Period

D 611 Aniline Point

D 664 Acid Number by Potentiometer Titration

D 847 Acidity in Benzene, Toluene, Xylene, Solvent Naphtha and Aromatics

D 848 Acid Wash Color of Industrial Aromatic hydrocarbons

D 849 Copper Corrosion in Benzene

D 850 Distillation

D 852 Solidification Point of Benzene

D 853 H2S & SO2

D 874 Sulfated Ash from Lubricating Oils and Additives

D 974 Acid and Base Number by Color Indicator Titration

D 975 Specification of Diesel Fuel Oils

D 976 Cetane Index (Calculation)

D 1078 Distillation

D 1125 Conductivity

D 1160 Vacuum Distillation

D 1209 Color of Clear Liquids (PT-CO Scale)

D 1293 pH

D 1296 Odor of Volitile Solvents and Dilutents

D 1298 Hydrometer method - Density Relative Density (Specific Gravity / API)

D 1319 Hydrocarbon Type in Liquid Petroleum Products by Fluorescent Indicator Adsorption (FIA)

D 1322 Smoke Point of Kerosene and Aviation Turbine Fuel

D 1353 Non Volatile Matter in Solvents

D 1363 Permanganate Time of Acetone and Methanol - Wall wash samples

D 1364 Water (KF)

D 1401 Water Separability of Petroleum Oils and Synthetic Fuels

D 1405 Heat of Combustion

D 1464 Water (KF)

D 1493 Solidification Point - Industrial Organic Chemicals

D 1500 ASTM Color of Petroleum Products

D 1613 Acidity in Volatile Solvents and Chemical Intermediates

D 1614 Alkalinity in Acetone

D 1722 Hydrocarbon / Water Miscibility of water soluble Solvents - Methanol wall wash

D 1796 Water and Sediments in Fuel Oil by Centrifuge Method.

D 2090 Appearance

D 2109 Non Volatile Matter in Halogenated Organic Solvents and Ad Mixtures

D 2110 pH

D 2119 Aldehydes in Styrene

D 2121 Polymer in Styrene

D 2163 Analysis of LPG and Propane by GC

D 2274 Oxidation Stability

D 2306 C8 Hydrocarbon Analysis - GC

D 2340 Peroxide in Styrene

D 2360 Trace Impurities in Mixed Xylene - GC

D 2386 Freezing Point

D 2500 Cloud Point

D 2622 Sulfur by X-Ray Spectrometry

D 2624 Electrical Conductivity of Aviation and Distillate Fuel

D 2709 BS&W - Water and Sediments in Middle Distillate Fuels.

D 2989 Acidity - Alkalinity of Halogenated Solvents - Acetone

D 2989 Alkalinity

D 3120 Sulfur - Trace Quantities of Sulfur using a micro coulometer

D 3227 Mercaptan Sulfur

D 3230 Salt in Crude Oil

D 3240 Undissolved water in Aviation Turbine Fuels

D 3241 Oxidation Stability JFTOT

D 3242 Acidity in Aviation Fuels

D 3246 Total Sulfur

D 3338 Heat of Combustion

D 3606 Determination of Benzene and Toluene in Gasoline - GC

D 4006 Water in Crude by Distillation

D 4007 Water and Sediments in Crude Oil by Centrifuge Method.

D 4052 Density and Relative Density of Liquids by Digital Density Meter

D 4176 Water and Particulate Contamination in Distilled Fuels (Haze Reading -Visual Appearance)

D 4294 Sulfur - by X-Ray

D 4376 Benzene - GC

D 4529 Heat of Combustion

D 4530 Determination of Carbon Residue (Micro Method) & 10% Bottom

D 4590 Inhibitor (TBC), ppm in Styrene

D 4737 Cetane Index (Calculation)

D 4740 Compatibility / Cleanliness

D 4790 Acid Wash Color

D 4807 Sediments in Crude by Membrane Filters.

D 4814 Drivability Index (V/L Ratio - Calculations)

D 4814 Test Determination for Corrosiveness of Sulfur from Petroleum Products using Silver Strip Test

D 4815 Determination of Oxygenates in Gasoline by GC

D 4860 Free water and Particulate Contamination in Mid Distillate Fuels.

D 4928 Water by Karl Fisher (Coulometric)

D 4952 Doctor Test

D 5002 Density and Relative Density of Crude Oils by Digital Density Meter

D 5186 Determination of Aromatic Contents & Polynuclear Aromatics in Diesel by SFC

D 5191 RVP Mini Method

D 5386 Color - Hunter. PT-Co

D 5452 Particulate Contamination (Filtration)

D 5453 Sulfur by Antex

D 5501 Determination of Ethanol Content of Denatured Fuel Ethanol by GC

D 5569 Aromatics GC-MS and DCPD

D 5571 Cloud Point (Auto)

D 5590 Determination of Oxygenates in Gasoline by OFID - GC

D 5705 Measurement of Hydrogen Sulfide in the Vapor Phase of Residual Fuel Oil - (Draeger Tube)

D 5769 Determination of Benzene, Toluene and Total Aromatics by GCMS

D 5972 Freeze Point (Automatic Phase Method)

D 6045 Tristimulus Color - Color of Petroleum Products by Automatic Tristimulus Method

D 6217 Particulate Contamination (Filtration)

D 6304 Water by Karl Fisher (Coulometric)

D 6371 Cold Filter Plugging Point (CFPP)

D 6423 pHe of Ethanol, Denatured Fuel Ethanol and Fuel Ethanol

D 6468 High Temperature Stability

D 6550 Determination of Olefin Content in Gasoline by SFC

D 6560 Asphaltene

E 70 pH of Aqueous Solution

E 200 Standard Preparations

E 203 Water by Karl Fisher (Volumetric) Hydrant Comp 5, Hydrant Solvent

E 299 Peroxide, ppm

E 394 Iron

E 411 Carbonyl compounds

E 769 Odor in Methanol, Ethanol, N-Propanol, Isopropanol

E 1064 Water by Karl Fisher (Coulometric)

EN 116 Cold Filter Plugging Point (CFPP 6371)

EN ISO 2719 Flash Point ( D93)

EN ISO 3104 Kinematic Viscosity, 40ºC (D445)

EN ISO 5165 Cetane Number (D613)

EN ISO 20846 Sulfur (D5453)

EN ISO 23015 Cloud Point (D2500)

EN 12205 Oxidation Stability

EN 12662 Particulate Contamination (Filtration) (D6217)

EN 14112 Oxidation Stability (D2274)

IP 143 Asphaltene (D6564)

IP 470 Metals by Flux Fusion

ISM Octel F-21 Oxidation Accelerated Stability (DuPont)

UOP 163 Measurement of Hydrogen Sulfide in the Liquid Phase & Mercaptan Sulfur.

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