*

HUSSEIN HAMAD Ph.D

Lebanese University

Faculty of sciences section V, Nabatieh, Lebanon

Platform of Research and Environmental Sciences Analysis

(PRASE), Doctoral school, Beirut, Lebanon

Email: admy2z@r.postjobfree.com;

admy2z@r.postjobfree.com

QUALIFICATIONS

I have a doctorate in philosophy in material and analytical chemistry and I have Master degree in bioanalytical chemistry. I have experienced in surface modification, fictionalizations and enzyme immobilizations. I have a broad knowledge in almost all analytical techniques which are required to conduct research and analysis. I have intensive experience with analytical methods such as HPLC, GC, and CE. I am able to function well within multidisciplinary teams. RESEARCH INTERESTS

“Synthesis and characterization of catalysis based on mesoporous materials and environmental application” This is a new procedure for synthesis of mesoporous materials MSU-type and SBA-15, and functionalized mesoporous materials. This method consists of the direct incorporation of active catalysts heteropolyacid, such as tungstophosphoric (H3PW12O40) and platinum (H2PtCl6), in the mesoporous solid. Also these materials can be modified with chelating agents such as EDTA, both of them will be used in environmental applications.

“Methods for enzyme (trypsin) immobilization on a solid support for peptide mapping by chromatography” This method for immobilizing enzymes by covalent bond via different spacers such as glutaraldehyde on different supports. Optimization of the enzyme quantity for higher activity, quantification and kinetic (KM and VM) will be studied. In the second part, digestion test in a microreactor will be achieved EDUCATIONAL BACKGROUND

2003 – 2006 Ph.D. Material and Analytical Chemistry, University of High Alsace (UHA),

Mulhouse, France.

2000 – 2002 Master Degree M.Sc., Analytical Chemistry University of Montréal(UdeM),

Québec, Canada.

1996 – 1999 B.Sc. Chemistry,

University of Québec at Montréal (UQAM),

Québec, Canada

1992 – 1995 DEC in Dental Technicien

2

Collège Edward Mont-Petit

Québec, Canada.

1987 – 1989 Preparation for senior academic years, Faculty of The Sciences I,

Beirut, Lebanon

PROFESSIONAL EXPERIENCE

2007-2014 Assistant Professor (Part Time)

Lebanese International University (LIU),

Faculty of Arts and Science, Department of

Biological and Chemical Sciences, Beirut,

Lebanon

Responsibilities: I am the Coordinator for Analytical Chemistry (CHEM260), and it Laboratory. This involves coordinating between instructors in all campuses, insuring that the course syllabus meets standards.

Teaching: I currently teach the following courses: Quantitative Analytical Chemistry (Phar205), General Chemistry II (CHEM200), Analytical Chemistry (CHEM260) and Food Chemistry (FDSC370) 2007 -Still Assistant Professor (full Time)

Lebanese University (LU),

Faculty of Science V, Department of Chemistry

and Biochemistry, Beirut, Lebanon

Responsibilities: I am the Coordinator for Analytical and bio analytical chemistry courses that I teach (see teaching section) and it Laboratory. This involves setting up common exams which satisfy and unify all instructors.

Teaching: I currently teach the following courses: Analytical techniques for biochemists (BIOC301); Analytical chemistry II: Separation methods (CHEM337); Analytical chemistry II: Optics and instrumentations (CHEM312) and Analytical chemistry I (CHEM229) I demonstrate the following laboratories: Analytical chemistry II (CHEM342); Analytical chemistry III (CHEM343): Bioanalytical chemistry II (BIOC341). 2009 – Still Platform of Research and Environmental Sciences Analysis (PRASE), Doctoral school,

Beirut, Lebanon

Responsibilities : I am currently involved in the collaboration with PRASE geochemistry research group. I am responsible for the analysis on the NMR & HPLC techniques. Feb.2008 – Oct. 2008

Manager at Al Bahar International company,

Technocrete division (paint & decorative materials) Ghazieh, Lebanon,

Responsibilities Manager, and installation of analysis techniques 2002-2005 Chemistry Instructor (part time)

Institute of Technology,

Jwaya, Lebanon

Teachings Teaching and demonstrating general and analytical chemistry courses and Laboratories for the 1st and 2ed year chemistry; medical laboratory

2002 – 2003

Chemistry Instructor

Cadmous College,

Tyr, Lebanon

3

Teaching Teaching chemistry to the secondary classes: S.V, S.G and S.E 1999 – 2001 Teaching and demonstrator for undergraduate courses and Laboratory University of Montréal

Quebec Canada

Teaching

I taught the following course: Analytical techniques for biochemists (CHIM2172); Analytical chemistry II: Separation methods (CHEM337); Analytical chemistry II: Optics and instrumentations (CHEM312) and Analytical chemistry I (CHEM229) I demonstrate the following laboratories: Analytical chemistry II (CHEM342); Analytical chemistry III (CHEM343): Bioanalytical chemistry II (BIOC341). Responsibilities Teaching assistant as lab. Demonstrator for the following courses: Analytical chemistry for biochemists (CHM1978). Instrumental Analysis for Chemists (CHM2971) and the improvement for the following techniques: HPLC, GC, Fluorimetry. Also, Co-supervision (with Prof. Waldron) of two summer students’ research projects 1995 – 2000 Technician in dentistry field, with Jacinthe Marcil, Denturologist Montréal, Canada

Responsibilities Fabrication and finishing partial and complete denture prosthesis RESEARCH ACTIVITIES

2009-still Platform of Research and Environmental

Sciences Analysis (PRASE), Doctoral school,

Beirut, Lebanon

Unité de recherche Sols, Eaux, Déchets et

Ressources (SEDR)

Research involves the removal of heavy

metal using mesoporous material and

activated carbon.

Under my supervision many M2 students

2011-still Platform of Research and Environmental

Sciences Analysis (PRASE), Doctoral school,

Beirut, Lebanon

Collaboration with Poitiers University in

France- Enviromental Chemistry

Research involves the removal of heavy

metal using mesoporous material and

activated carbon

Under my supervision there is a Ph.D.

Candidate (joint project).

UQAM university (Montréal) and the National

Institute of Scientific Research (INRS)

4

2003 – 2006 University of High Alsace (UHA),

Ph.D In material and analytical chemistry

R&D in the Synthesis and characterization

of catalysis based on mesoporous materials

and environmental application in NOx

reduction

2000-2002 University of Montreal Master degree (M.Sc) in analytical chemistry, I devepolled three Methods for

enzyme (trypsin) immobilization on a

solid support for peptide mapping by

capillary electrophoresis

PUBLICATIONS

A. Journal Papers:

1. The applicability of as synthesized mesoporous carbon CMK-3 as a heavy metals adsorbent: application to real water samples; Energy Sources, Part A: Recovery, Utilization, and Environmental Effects, Zeinab Ezzeddine, Isabelle Batonneau- Gener, Yannick Pouilloux, Hussein Hamad & Zeinab Saad (2019). https://doi.org/10.1080/15567036.2019.1663301

2. Synthetic Nax Zeolite as a Very Efficient Heavy Metals Sorbent in Batch and Dynamic Conditions, colloid and interfaces, Zeinab Ezzeddine, Isabelle Batonneau-Gener, Yannick Pouilloux, Hussein Hamad and Zeinab Saad (2018) 3. • Removal of methylene blue by mesoporous CMK-3: Kinetics, isotherms and thermodynamics Zeinab Ezzeddine, Isabelle Batonneau-Gener, Yannick Pouilloux, Hussein Hamad; Journal of Molecular Liquids, In Press, Accepted Manuscript, Available online 3 September (2016)

4. • An insight into the removal of Cu (II) and Pb (II) by aminopropyl-modified mesoporous carbon CMK-3: Adsorption capacity and mechanism, Hussein Hamad; Zeinab Ezzeddine, Fatima Lakis, Hassan Ramal, Mortada Srour, Akram Hijazi Material Chemistry and Physics, Materials Chemistry and Physics, Volume 178, 1 August (2016), Pages 57-64 5. • A novel modification and selective route for the adsorption of Pb2+ by oak charcoal functionalized with glutaraldehyde Hussein Hamad;Zeinab Ezzeddine, Samah Kanaan, Fatima Lakis, Akram Hijazi, Mhamad-Aly Moussawi Mortada Srour, Advanced Powder Technology, 27 (2016) 631–637 6. • ‘Divalent Heavy Metals Adsorption onto Different Types of EDTA-Modified Mesoporous Materials: Effectiveness and Complexation Rate’. Zeinab Ezzeddine, Isabelle Batonneau-Gener, Yannick Pouilloux, Hussein Hamad, Zeinab Saad, Veronique Kazpard. Microporous and Mesoporous Materials, Volume 212, August( 2015), Pages 125-136 7. • Mhamad-Aly Moussawi, Akram Hijazi, Hussein Hamad, Hassan Rammal, wassim rammal, mohamad alameh, daoud naoufal; biosorption of methylene blue from waste water using 5

scabiosaprolifera (carmel daisy); world journal of pharmaceutical research, volume 3, issue 8, (2014) 45-56.

8. Daoud Naoufal, Zahra Laila, Ogaritte Yazbeck, Hussein Hamad, Ghassan Ibrahim, Riman Aoun, Ali Safa, Mohieddine ELJamal and AliKanj; Synthesis, characterization and mechanism of formation of 6-substituted nido-B10H13 decaboranes by the opening reaction of closo-decahydrodecaborate

[B10H10]2− cage, Main Group Chemistry 12 (2013) 39–48 9. Joumana Toufaily, Bachar Koubaissy, Lina Kafrouny, Hussein Hamad, Patrick Magnouxc, Leila Ghannam, Ali Karout, Hassan Hazimeh, Ghinwa Nemra, Moustafa Hamieh, Nawal Ajouz, Tayssir Hamieh. Functionalization of SBA-15 Materials for the Adsorption of Phenols, from Aqueous Solution, Central European Journal of Engineering, Cent. Eur. J. Eng. (2012) 3 (1) 126-134 10. Hussein Farhan, Hassan Rammal, Akram Hijazi, Hussein Hamad and Bassam Badran; Photochemical screening and extraction of polyphenol from stems and leaves of Lebanese Euphoria macrolada extraction schyzoceras Bios; Annals of Biological Research, (2012), 3 (1):149- 156

11. H. Farfan, H. Ramal,A. Hijazi,H Hamad, A Daher, M. Reda, B. Badran; In vitro antioxidant activity of ethalonic and aqueous extracts from crude malva prvifloral grown in Lebanon, Asian Journal of Pharmaceutical and Clinical Research Vol 5, Suppl 3, 2012 12. C. Dartiguenave, H. Hamad and K.C. Waldron, “Immobilization of Trypsin onto 1,4 Diisothiocyanatobenzene-Activated Porous Glass for Microreactor–Based Peptide Mapping by Capillary Electrophoresis Part I: The Immobilization Procedure and Effect of Calcium Ions”, Analytica chimica acta vol. 663, no2, (2010), pp. 198-205 13. Hamad, Hussein; Hamieh, Tayssir; Mahzoul, Hakim; Toufaily, Joumana (2008). NOx reduction over MSU molecular sieves catalysts obtained by direct incorporation of platinum and 12- tungstophosphoric acid H3PW12O40. DeNOx Catalysis, Advanced Powder Technology, Volume 19, Number 3, (2008), pp. 231-252(22).

14. Hussein Hamad, Michel Soulard, Bénédicte Lebeau, Joël Patarin, Tayssir Hamieh, Joumana Toufaily and Hakhim Mahzoul (2007). A new way for DeNOx catalyst preparation: Direct incorporation of 12- Tungstophosphoric Acid H3PW12O40 and Platinum into Mesoporous Molecular Sieves material Journal of Molecular Catalysis A: Chemical, Volume 278, Issues 1-2, 14 December 2007, Pages 53-63. 15. Hussein Hamad, Tayssir Hamieh, Joumana Toufaily and Hakhim Mahzoul. Synthesis and characterization of MSU molecular sieves catalysts obtained by direct incorporation of platinum and 12-tungstophosphoric acid H3PW12O40, Advanced Powder Technology, Volume 19, Number 2, (2007), pp. 131-151.

16. J. Toufaily, M. Soulard, J.-L. Guth, J. Patarin, T. Hamieh, M. Kodeih, D. Naoufal, H. Hamad (2007). Synthesis and characterization of new catalysts formed by direct incorporation of heteropoly acids into organized mesoporous silica Colloids and Surfaces A: Physicochemical and Engineering Aspects, Volume 316, Issues 1-3, 5 March (2008), Pages 285-291 17. J. Toufaily, J-L. Guth, M.Soulard, J. Patarin, H. Hamad, T. Hamieh RMN du 31P et mesure du temps de relaxation de l’acide 12-tungstophosphorique incorporé par synthèse directe dans une charpente silicique mésoporeuse Journal de Physique IV., (2005)124, 69-74 18.

B. Book

Chapters:

H. Hamad, Reduction des NOx par le propène sur des catalyseurs obtenus par incorporation directe de H3PW12O40 et Pt dans des silices mesoporeuses de type MSU et SBA-15.Thesis presented and accepted on April 7th 2006, in fulfillment of the requirements for the degree of Doctor of Philosophy in material, Chemistry at UHA University, FRANCE.

C. Conference

Papers:

1. Lead (II) Removal by EDTA-Modified Mesoporous KIT-6. Zeinab Ezzeddine, Isabelle Batonneau- Gener, Yannick Pouilloux, Hussein Hamad, Zeinab Saad. 11ème Symposium International« Environnement, Catalyse et Génie des Procédés » (ECGP’11), Lille, France. 26 - 28 juin 2013.(Oral) 6

2. Divalent Heavy Metals Adsorption EDTA Modified Mesoporous Materials. Zeinab Ezzeddine, Isabelle Batonneau-Gener, Yannick Pouilloux, Hussein Hamad, Zeinab Saad, Veronique Kazpard. Lebanese Association for Advancement of Science (LAAS) Lebanese university May 2014 3. Divalent Heavy Metals Adsorption on NaX Zeolite and EDTA Modified SBA-15: A Comparative Study. Zeinab Ezzeddine, Isabelle Batonneau-Gener, Yannick Pouilloux, Hussein Hamad, Zeinab Saad. 30th annual reunion of Groupe Française des Zéolithes. Ile de Ré, France. 19 – 21 Mars 2014. 4. Adsorption du cuivre sur silice mésoporeuse SBA-15 modifiée. Zeinab Ezzeddine, Isabelle Batonneau-Gener, Yannick Pouilloux, Hussein Hamad, Zeinab Saad. Association Française de l’Adsorption (AFA). Paris (Jussiue),France. 14-15 Mai 2013. 5. Copper Adsorption onto NaX Zeolite . Zeinab Ezzeddine, Isabelle Batonneau-Gener, Yannick Pouilloux, Hussein Hamad, Zeinab Saad, Veronique Kazpard. Lebanese Association for Advancement of Science (LAAS), LAU, Beirut, Lebanon. 5-6 April 2013. 6. H. Hamad, M. Soulard, B. Lebeau, J. Patarin, T. Hamieh, H. Mahzoul, J. Toufaily (2006) NOx reduction over H3PW12O40 and Pt catalysts MSU type materials (CSM5: Cinquième Colloque Franco-Libanais sur la Science des Matériaux, Mai 17- 19, 2006, Beyrouth, Liban) 7. H. Hamad, M. Soulard, B. Lebeau, J. Patarin, T. Hamieh, H. Mahzoul, J. Toufaily (2006) Synthesis and characterization of MSU type material containing platinum (Pt) and 12-tungstophosphoric acid

(H3PW12O40) (CSM5: Cinquième Colloque Franco-Libanais sur la Science des Matériaux, Mai 17- 19, 2006, Beyrouth, Liban)

8. J. Toufaily, J-L. Guth, M. Soulard, J. Patarin, H. Hamad, T. Hamieh RMN of the 31P and measure of time of acid 12-tungstophosphorique relaxation incorporated by direct synthesis in a framework silicique mésoporeuse (CSM4: Quaterième Colloque Franco- Libanais sur la Science des Matériaux, Mai 26-28, 2004, Beyrouth, Liban) 9. K.C. Waldron, C. Dartiguenave, I. Migneault, H. Hamad, M.J. Bertrand and J. Vinh (2003) “An Evaluation of Trypsin Immobilization Methods With or Without a Solid Support for Electrophoretic, Chromatographic and Mass Spectrometric Peptide Mapping”, The 39th IUPAC Congress and The 86th Conference of the Canadian Society for Chemistry, Ottawa, Ontario (Canada), August 10-15, 2003. 10. I. Migneault, C. Dartiguenave, H. Hamad, M.J. Bertrand and K.C. Waldron (2003) “Trypsin Immobilization by Two Glutaraldehyde Methods for Peptide Mapping by Capillary Electrophoresis and Liquid Chromatography”, The 39th IUPAC Congress and The 86th Conference of the Canadian Society for Chemistry, Ottawa, Ontario (Canada), August 10-15, 2003. 11. I. Migneault, C. Dartiguenave, H. Hamad, Ka.C. Waldron, M.J. Bertrand and J. Vinh (2003)

“Comparison of Trypsin Immobilization Techniques with or Without a Solid Support for Peptide Mapping”, ASMS2003: The 51st Annual Conference on Mass Spectrometry and Allied Topics, Montreal, Quebec (Canada), June 8-12, 2003.

12. C. Dartiguenave, K.C. Waldron, H. Hamad, C. Mikonio, V. Labas and J. Vinh (2003) “Optimization of Enzyme Immobilization Techniques and Miniaturized Peptide Mapping Devices for Structural Proteomics Applications”, HPCE 2003: The 16th International Symposium on Microscale Separations, San Diego, California (USA), January 17-22, 2003.

13.

K.C. Waldron, C. Dartiguenave, H. Hamad, C. Mikonio, V. Labas and J. Vinh (2002) “Optimization of Enzyme Immobilization Techniques and Miniaturized Peptide Mapping Devices for Structural Proteomics Applications”, The 1st World Congress of HUPO (Human Proteome Organization), Versailles (France), November 21-24, 2002.

14. Catherine Dartiguenave, Hussein Hamad and Karen C. Waldron, “Evaluation of a Microreactor Composed of Wide Bore Fused Silica Capillary packed with Trypsin Immobilized via DITC on Controlled Pore Glass”, The 13th Annual Frederick Conference on Capillary Electrophoresis (FCCE), Frederick, Maryland (USA), October 21-22, 2002

15. Catherine Dartiguenave, Hussein Hamad and Karen C. Waldron, “Optimization of an Enzyme Microreactor : Three Immobilization Procedures for Trypsin on Controlled Pore Glass”, HPLC2002: The 26th International Symposium of High Performance Liquid Phase Separations and Related Techniques, Montréal, Québec, (Canada), June 2-7, 2002. 16. H. Hamad, C. Dartiguenave and K.C. Waldron (2001) “Investigation of Enzyme Immobilization Methods on Controlled Pore Glass (CPG) for Microreactor-based Peptide Mapping”, The 84th Canadian Society for Chemistry Conference, Montréal, Québec (Canada), May 26- 30, 2001. 7

17. H. Hamad, C. Dartiguenave, H. Cong and K.C. Waldron (2001) “Comparison of Three Techniques for Enzyme Immobilization on Controlled Pore Glass (CPG) for Microreactor-based Peptide Mapping”, The 12th Annual Frederick Conference on Capillary Electrophoresis (FCCE), Frederick, Maryland

(USA), October 15- 16, 2001.

18.

AFFILIATIONS

Reviewer for Journal of Molecular Catalysis A: Chemical SOFTWARE

• Software: Microsoft office,(word, excel, power point, ….), Endnote,

Origin,

internet tools,

ACDLab

• Languages : Basic knowledge in C++,

LANGUAGES

1- Arabic

2- English

3- French

REFERENCES

Prof. Karen C. Waldron (M.Sc.

Supervisor).

Université de Montréal

Tel : 1-514-***-****

E.mail:admy2z@r.postjobfree.com

Prof. Joël Patarin (Ph.D.

Supervisor)

Université de Haute Alsace

Tel : 33 (3) 89 33 68 80

E.mail: admy2z@r.postjobfree.com

Prof. Daniel Bélanger (Post Doc

Supervisor)

NanoQam, Université UQAM, Tel :

1-514-***-****, ext.3909

E.mail:admy2z@r.postjobfree.com

Contact this candidate