Analytical Chemist

Matthew Mullaney

**** *. ******* ******

H: 302-***-****

Wilmington, DE 19801

************@*******.*** C: 610-***-****

PROFILE

Skilled Analytical Chemist with comprehensive applied background in HPLC,

IC and GC separations and wet chemical analysis. Experienced in analytical

method development, validation and transfer using these techniques under

cGMP, cGLP and ISO 17025 guidance. Collaborative team member in active

analytical service organizations.

PROFESSIONAL EXPERIENCE

Jacobs Engineering (ATSS), Applied Science Test Division, Aberdeen Proving

Grounds, MD 2010 - 2013 Scientist III

. Developed and conducted 8 chemical assays for analytes in difficult

matrices on routine basis.

. Evaluated experimental data, performed literature research, improved

and validated 4 new analytical procedures related to toxic vapor

emissions.

. Purchasing lead for Waters Acquity UPLC, Shimadzu Prominence IC and

Metrohm Titrino.

Nutramax Laboratories, Analytical Chemistry Laboratory, Edgewood, MD

2008 - 2010

Analytical Scientist IV

. Developed and validated 5 analytical methods for active ingredients

and impurities within marine oil and anti-inflammatory products.

. Assisted 5 product development studies; established GC, HPLC, UPLC,

and Karl Fischer titration analyses.

. Wrote 7 analytical methods, 7 validation and transfer protocols and 7

validation reports to support QC.

ASDI, Inc., Pharmaceutical Research Services, Newark, DE

2008

Senior Scientist -Temporary Assignment

. Verified compound identity and purity for more than 2200 samples via

NMR, LC-MS and GC-MS analyses.

. Executed more than 3000 1H, 13C, 1H-1H COSY and 1H-13C HETCOR NMR

experiments for structure verification.

. Ensured NMR data quality for 6 system users by creating and

implementing maintenance and calibration schedules, limiting NMR down

time to less than 4% of total scheduled usage time.

West Pharmaceutical Services, West Monarch Labs, Lionville, PA

2006 - 2008

Senior Chemist

. Developed and validated 12 trace-level analytical methods for

leachable/extractable substances in West products used by external

customers.

. Supported internal and external customers; planned and directed 3

analytical investigations.

. Wrote 12 analytical methods, validation protocols and validation

reports.

. Confirmed instrument usability by qualifying and maintaining HPLC and

IC instruments.

Rohm & Haas Company, Consumer Industrial Specialties, Spring House, PA

2005 - 2006

Scientist

. Created 4 HPLC analyses for biocides in treated wood and marine

antifoulant paints.

. Purchasing lead for Rapid Resolution Agilent 1200 HPLC system to

increase analysis throughput.

. Provided current, relevant documentation by writing 3 SOPs and 4

testing procedures.

. Established HPLC usability by performing qualification and

preventative maintenance.

Merck & Company, Inc., West Point, PA

Staff Chemist, Bioprocess Research and Development

2001 - 2005

. Supported product development for 4 nascent vaccines through

development and validation of 9 HPLC and IC methods for amino acids,

proteins, saccharides, cations, anions, water-soluble vitamins and

organic acids.

. Guaranteed current documentation by writing/updating 4 SOPs and 9

testing procedures.

. Purchasing lead for Trace GC and Trace DSQ GC-MS instrumentation to

enhance laboratory capabilities.

Page 2

************@*******.*** Matthew

Mullaney

Merck & Company, Inc., West Point, PA

Analytical Chemist/Senior Analytical Chemist, Pharmaceutical Testing

Laboratory 1999 - 2001

. Performed routine stability and release testing/documentation for more

than 300 product lots.

. Assisted in raw material release for manufacture by executing JP, EP,

BP and USP testing methodologies.

. Trained 6 personnel in use of Waters HPLC, HP 8452A Diode Array UV-Vis

Spectrophotometer and Brinkman 702SM Titrino.

EDUCATION AND PROFESSIONAL DEVELOPMENT

Duquesne University, Pittsburgh, PA

M.S., Chemistry

. Thesis Title: 1- and 2-Dimensional Proton, Carbon-13, and Platinum-195

NMR Studies of Pt(EDTA)Cl2 in D2O Solution and Structural

Characterization of Several Fe(III) Tris-(2-pyridylmethyl)-amine

Complexes, Dec 1996.

. As adjunct lecturer, taught general, nursing and senior inorganic

chemistry laboratories, conducted recitation sessions in general and

nursing chemistry, wrote and graded quizzes and laboratory exams.

University of Pittsburgh, Pittsburgh, PA

B.S., Chemistry

. Minors in Biology and Mathematics.

. Laboratory Technician for 3 years in the Department of Molecular

Immunology.

. Participated in 2 consecutive SERS Internships at Argonne National

Laboratory.

Course Title and Sponsor

Statistical Analysis of Laboratory Data, American Chemical Society.

Experimental Design for Productivity and Quality in R&D, American Chemical

Society.

Alliance HPLC System Operation and Performance Maintenance, Waters Connection

University.

Gas Chromatography, Fundamentals, Troubleshooting, and Method Development,

American Chemical Society (Hands-on Course).

How to Develop Validated HPLC Methods: Rational Design with Practical Statistics

and Troubleshooting, American Chemical Society.

Empower Software Advanced Topics with Lab, Waters Connection University.

Effective Management of Chemical Support Laboratories, American Chemical

Society.

PUBLICATIONS

Mullaney, Matthew; Chang, Shih-Chi; Norman, Richard E.. Crystal Structure

of dichloro(ethylenediaminediacetic

acid-N,N')Platinum(II). Inorg. Chim. Acta, 265, (1997), pp. 275-278.

Fleming, Frazier; Hussain, Zahid; Mullaney, Matthew; Norman, Richard E.;

Chang, Shih-Chi. (8R, 8aS)-Indolizidine-1-spiro-2'-(1',3'-dithiane)-8-

carbonitrile. Acta Crystallographica, 52 Sec. C (1996) pp. 2849-2851.

Tzou, Ji-Ren; Mullaney, Matthew; Norman, Richard E.; Chang, Shih-Chi.

Hexakis(dimethyl sulfoxide-O)iron(III)Trinitrate. Acta Crystallographica,

51 Sec. C (1995) pp. 2249-2252.

PROFESSIONAL AFFILIATIONS

American Chemical Society, 1993-Present, Chromatography Forum of Delaware

Valley, 2000-present

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