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Development ProcessEngineer

Location:
Chicago, IL
Posted:
March 28, 2014

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Resume:

Phone 773-***-****, ***

Chicago, Illinois *** ***1

Email:

*********@********.***

Analytical Chemist

Functional Summary Objective: PhD Process Analytical Chemist with 10+ years

industrial research experience in Petrochemical,

Pharmaceutical and Biofuels chemistries. Desires lab

management customer technical service position in industry.

Skills list: Analytical HPLC and LC TOF method development,

documentation, implementation and customer training. FTIR

Process Mass Spec and Laser based trace gas analyses. Has

authored method development protocols and reports, new

equipment operating manuals and developed software for

automated chemical analysis. Strong points are technical

knowledge, excellent verbal and PC skills, proven teaching

ability, customer support and competitive product research.

Has maintained analytical instruments.

Has taught graduate level spectroscopy and biochemistry

classes, undergraduate organic general and physical chemistry

classes.

HPLC, LC TOF, ICP, FTIR Method Development, mass spectroscopy,

capillary gas chromatography, ligand-binding assays, GC / MS,

NMR, IR, FTIR, Raman, UV, Circular Dichroism, spectral

analysis, ion chromatography, size exclusion chromatography,

TLC, dialysis, ultracentrifugation, Chemometrics, partial

least squares, nonlinear modeling techniques as neural

networks, NeuralWare, Galactic Software, CAMO Unscrambler.

CCD Electro optic system design and spectroscopic sensor

implementation. Expert systems development using Gensym g2,

Visual Basic. Skill points are: critical thinking, creative

problem-solving, versatile statistical analyses, strong

technical knowledge, excellent verbal skills, proven teaching

ability. Has authored operating manuals and is computer savvy.

He is able to do clean up as well as perform the duties of

assigned work.

rience May 2010 - July 2012- Coskata Warrenville, Illinois

Senior Analytical Chemist

Reporting directly to the head of R&D: In charge of and

principal operator of Process Mass Spectrometer, FTIR, IR

Diode Laser Gas Analyses, LC TOF, HPLC DAD, FTIR, Headspace

GC/MS, ICP OES of all materials for anaerobic fermentations.

Evaluated syn gas content in relation to treatment for ppm and

ppb levels of gases quantitation, qualitative. Optimized

methods for HPLC time of flight mass spectrometry

determination of trace levels of amino acids. Identified the

need to have in house ICP for process control, replacing

expensive and time delayed external lab analyses. Specified

and recommended ICP OES for trace metals determinations for

Coskata. Identified new metabolites from isolated organisms,

conducted isotopic tracer studies with Headspace GC / MS.

Evaluated Raman and other technologies for gas analyses.

Analytical troubleshooting fermentors, process mass

spectroscopy.

January 2009 - May 2010 - North Park University Chicago,

Illinois

Professor of Chemistry

Teaching of Chemistry classes and labs. Includes twelve hours

classroom time and four hours of laboratory instruction.

Course curriculum design and evaluation design for chemistry

courses.

January 2008 May 2010 - National University of Health

Sciences Lombard, Illinois

Professor of Chemistry

Teaching of Organic Chemistry classes and labs. Teaching of

Pharmacology. Included twelve hours classroom time and four

hours of laboratory instruction. Collaborative research and

program direction. Course curriculum design and evaluation

design for organic chemistry courses.

Aug 2007- June 2008- Elmhurst College Chicago, Illinois

Professor of Chemistry

Teaching of General Chemistry classes and labs. Includes four

hours classroom time and four hours of laboratory instruction.

Course curriculum design and evaluation design for general

life sciences chemistry courses.

March - May 2007 - American Indian Health Chicago, Illinois

Diabetes Coordinator

Community Health / Diabetes Coordinator for American Indian

focused clinic. Co Authored application for certification as

a center for diabetes care for Native Americans to Indian

Health Services. Managed one certified dietitian and one

community health care worker as part of the diabetes team.

Delivered Nursing care for diabetic patients utilizing the

nursing process standards of care and physician orders.

Fall 2006 Resurrection Medical Center Chicago, Illinois

Staff Nurse

Staff Nurse for Emergency Department at Resurrection Medical

Center. Deliver Nursing care utilizing the nursing process of

assessment, planning, implementation, evaluation and adhering

to establish policies procedures, standards of care and

physician orders. Computer entry of physician orders.

Fall 2001 - Spring 2005 East West University, Triton College,

Morton College, Illinois Institute of Technology, Roosevelt

University, Loyola University of Chicago: Chicago area,

Illinois

Adjunct / Part Time Professor of Chemistry

Teaching of General Chemistry, Spectroscopic Chemistry,

Organic and Biochemistry classes and labs. Course curriculum

design and evaluation design for all chemistry courses.

Purchasing and setup of entire laboratory for teaching of

chemistry, organic chemistry and biochemistry. Safe storage

of chemicals and adherence to protocols.

1997-2001 Gensym Corporation Arlington Heights, Illinois

Senior Consulting Engineer

Expert systems development for biochemical and drug

development projects. Worked with Pfizer, Inc. Research and

Development on automated HPLC / spectroscopic methods.

Intelligent software for chiral HPLC Method Development,

fermentation process management and control. Used techniques

of analytical chemistry for structural identification LC-MS,

GC-MS, Fluorescence, Fiber optic Near Infrared, FTIR and UV

spectrophotometry for small molecule isolation and ID.

1990-1996 UOP Des Plaines, Illinois

Project Coordinator: Instrumentation and Control Systems

Worked on a cross functional team concerned with the

optimization of existing UOP pilot plant operations, using

integrated spectroscopic analyzer and control system

development. Extensive use of Chemometric software and

spectroscopic instrumentation for fiber optic based near

infrared, Raman, Near Infrared and FTIR sensing of petroleum

process conditions. Received UOP R&D award for excellence as

a result of this effort.

Education 1985-1990 University of Illinois at Chicago Chicago, Illinois

Doctor of Philosophy, Physical Chemistry

Thesis work in Chiral Compound synthesis and NMR, Raman and

Infrared (FTIR) spectroscopic properties. Designed and

constructed a laser system for determination of Raman optical

activity with Semiconductor Diode array (CCD), pockels cell,

other electrooptic components. Was responsible for chiral

molecule synthesis, isolation and property determinations via

UV CD / 2-D NMR, VOA as FTIR, and ROA.

1983-1985 Illinois Institute of Technology Chicago, Illinois

Master of Science, Biophysical Chemistry

Isolation and spectroscopic characterization of Green Heme

from E. Coli

2005-2006 Loyola University of Chicago Chicago, Illinois

Bachelor of Science, Nursing

Accelerated Bachelor of Science Nursing program Marcella

Niehoff School of Nursing

Special interest areas MICU, ER, Telemetry units.

Publications:

"Intelligent Automation of High-Performance Liquid Chromatography Method

Development by Means of a Real-Time Knowledge-Based Approach", Ting Po I,

R. Smith, S. Guhan, Ken Taksen, Mark Vavra, Douglas Myers, Milton T. W.

Hearn, Journal Of Chromatography A, 972(1) (2002) 27-43 (Issue 10, 10

October 2002)

"Expert System Control of HPLC Method Development" [Tu-14], Myers and

Vavra at Lab Automation '99, Association for Laboratory Automation, Jan 30,

1999, San Diego, Ca.

"Raman Optical Activity of Small Molecules on a Spectrometer Assembled from

Commercially Available Components,"M. R. Vavra, T. A. Keiderling, in

"Eleventh International Conference on Raman Spectroscopy", ed. R. J. H.

Clark and D. A. Long, John Wiley, Chichester, U.K., p. 973-974, (1988).

"Simultaneous Raman and Cyclic Voltammetry Study of the Redox Behavior of

4,4'- Bipyridine on Silver", Therese Cotton, Mark Vavra Chemical Physics

Letters, Vol 106, No. 6, 491-497

"Proton NMR Spectroscopy of Sulfmyoglobin", Russell Timkovich, Mark Vavra,

Biochemistry, 1985, 24, 5189-5196.

"Spectroscopic Studies on Heme d in the Visible and Infrared", Mark Vavra,

Russell Timkovich, Flordeliza Yap, and Robert Gennis, Arch. Biochemistry

and Biophysics, Vol. 250, No. 2,Nov 1, pp 461-468.

Podium Abstracts Tuesday, September 29th Eurolab 1998

Intelligent HPLC Method Development Using Gensym's Lab Expert System

M. Vavra, Gensym Corporation, USA

EuroLabAutomation '98, Cambridge UK.

Metals Analyses

The ICP: Selection, purchase, Installation and commissioning and

operations, method development(s). Course WINLAB32 / ICP OES Optima Optima

Instrument Series with ICP WinLab32 Software-OES Course NO. 5010,

Inductively Coupled Plasma. The Perkin Elmer Optima 7000DV ICP-OES

instrument

The identification of significant savings in ownership and operation of a

ICP unit by company paid for the cost of the instrument in less than one

year. Developed methods for isolation of samples and analysis for [Co, Fe,

Cu, Mn, Zn, W, Mo, S, Na, K] in prepared samples.

Separations

The Agilent Electrospray Ionization LC TOF: Agilent R1874A 6210 LC/MS TOF

Techniques Dec 7 -10 2010, Schaumberg, Il.

Developed methods for vitamin analysis, amino acids quantitation.

Headspace analyzer G1888 (n), 6890N capillary GC, G3170A 5975B VL MSD

Fermentation broth qualitative analysis fermentors

HPLC Stack: Agilent 1200 series: Degasser, Quaternary Pump, ALS sample

injection, TCC heated column compartment, Diode array G1315D, Refractive

Index (RID)

Fermentation broth analysis, natural products analysis

6890N FID capillary GC

Fermentation broth quantitative analysis

FTIR

MKS 2030 LN2 MCT FTIR

Thermo Fisher Nicolet Antaris IGS FTIR

Evaluated process gas scrubbing and treatment for ppm levels of gases

quantitation, qualitative

Mass Spectroscopy:

Thermo Fisher Prima delta B with RMS 64

Quantitative gas component analyses, vital to fermentation controls

systems.

Process Instrumentation

Working with cross functional team of process engineers for the

specification of specialized on-line and at-line instrumentation for

process control for gasification including wood analysis by NIR, process

gas cleanup (as FTIR and process mass spec above), fermentor feed and

nutrient control, fermentor off gas analyses, product purity.



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